Faber K, Badaczewski F, Oschatz M, Mondin G, Nickel W, Kaskel S, Smarsly BM (2014)
Publication Type: Journal article
Publication year: 2014
Book Volume: 118
Pages Range: 15705-15715
Journal Issue: 29
DOI: 10.1021/jp502832x
Polymer-based silicon carbide-derived carbons (Si-CDCs) synthesized at temperatures from 600 to 1500 °C using different templating methods were characterized by wide-angle x-ray scattering (WAXS), Raman spectroscopy, and transmission electron microscopy (TEM). A recently developed advanced algorithm for fitting the whole WAXS data curve of non-graphitic carbons, that is, carbons with a polyaromatic sp2 structure, revealed fine details about the CDC microstructure on the level of the graphene layers. In particular, this approach allowed the quantification of disorder effects in the graphene stacks and the clarification of the peculiarity of CDCs. It is seen that, contrary to other types of carbons, almost no stacking of the sp2 layers occurs; that is, the stack height L
APA:
Faber, K., Badaczewski, F., Oschatz, M., Mondin, G., Nickel, W., Kaskel, S., & Smarsly, B.M. (2014). In-depth investigation of the carbon microstructure of silicon carbide-derived carbons by wide-angle X-ray scattering. Journal of Physical Chemistry C, 118(29), 15705-15715. https://doi.org/10.1021/jp502832x
MLA:
Faber, Kristin, et al. "In-depth investigation of the carbon microstructure of silicon carbide-derived carbons by wide-angle X-ray scattering." Journal of Physical Chemistry C 118.29 (2014): 15705-15715.
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