Smuda M, Stroeh J, Pienack N, Khadiev A, Terraschke H, Ruck M, Doert T (2022)
Publication Type: Journal article
Publication year: 2022
Book Volume: 330
Journal Issue: 12
DOI: 10.1039/d2dt02273g
The synthesis of intermetallic phases formed from elements with very different melting points is often time and energy consuming, and in extreme cases the evaporation of a reactant may even prevent formation completely. An alternative, facile synthesis approach is the reduction of metal salts in the polyol process, which requires only moderate temperatures and short reaction times. In addition, the starting materials for this procedure are readily available and do not require any special treatment to remove or prevent passivation layers, for example. Although the formation of intermetallic particles via the polyol process is an established method, little attention has been paid to the mechanism behind it. However, it is precisely a deeper understanding of the underlying mechanisms that would enable better and more targeted synthesis planning and product design. Taking the well-known formation of Bi
APA:
Smuda, M., Stroeh, J., Pienack, N., Khadiev, A., Terraschke, H., Ruck, M., & Doert, T. (2022). In situ investigation of the formation mechanism of α-Bi2Rh nanoparticles in polyol reductions. Dalton Transactions, 330(12). https://doi.org/10.1039/d2dt02273g
MLA:
Smuda, Matthias, et al. "In situ investigation of the formation mechanism of α-Bi2Rh nanoparticles in polyol reductions." Dalton Transactions 330.12 (2022).
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