The effect of the content of sodium in the obtaining of Na- β alúmina utilized the polymeric precursor method

Ruiz Madronero C (2011)


Publication Language: Spanish

Publication Type: Journal article, Original article

Publication year: 2011

Journal

Book Volume: 78

Pages Range: 190-195

Journal Issue: 165

URI: https://dialnet.unirioja.es/servlet/articulo?codigo=7761303

Abstract

In this work was utilized the Polymeric Precursor method to synthesis ceramic powders of Na + ­β­  alumina. We were interested in determinate the initial quantity from sodium precursor and its effect on crystalline phase obtained. Powders obtained were characterized using Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD)  and  Scanning  Electron Microscopy (SEM). The effect of the initial quantity of sodium in  the sample was very  important in the nature of the final product. If we used one stoichiometric quantity of NaOH, to obtain NaAl11O17 compound, we obtained α­-alumina as finish product (1450ºC). On the other hand, β­ alumina and/or Na2Al2xO3x­-1 were obtained in samples thermal treatment from 1000ºC to 1350ºC. When we used a higher quantity of NaOH, sample non­stoichiometric, a solid with NaAl11O17 as majority phase was obtained.  

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How to cite

APA:

Ruiz Madronero, C. (2011). The effect of the content of sodium in the obtaining of Na- β alúmina utilized the polymeric precursor method. Dyna-Colombia, 78(165), 190-195.

MLA:

Ruiz Madronero, Christhy. "The effect of the content of sodium in the obtaining of Na- β alúmina utilized the polymeric precursor method." Dyna-Colombia 78.165 (2011): 190-195.

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