Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy

Fritsch B, Hutzler A, Wu M, Khadivianazar S, Vogl L, Jank M, März M, Spiecker E (2021)

Publication Language: English

Publication Type: Journal article, Letter

Publication year: 2021

Journal

Nanoscale Advances Royal Society of Chemistry

Book Volume: 3

Pages Range: 2466 - 2474

Journal Issue: 9

URI: https://pubs.rsc.org/en/content/articlelanding/2021/NA/D0NA01027H

DOI: 10.1039/D0NA01027H

Open Access Link: https://pubs.rsc.org/en/content/articlepdf/2021/NA/D0NA01027H?page=search

Abstract

A significant electron-beam induced heating effect is demonstrated for liquid-phase transmission electron microscopy at low electron flux densities using Au nanoparticles as local nanothermometers. The obtained results are in agreement with theoretical considerations. Furthermore, the impact of beam-induced heating on radiolysis chemistry is estimated and consequences of the effect are discussed.

Authors with CRIS profile

Birk Fritsch Lehrstuhl für Elektronische Bauelemente Andreas Hutzler Lehrstuhl für Elektronische Bauelemente Mingjian Wu Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung) Saba Khadivianazar Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden Lilian Vogl Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden Michael Jank
Martin März
Erdmann Spiecker Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung)

Additional Organisation(s)

Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung) Interdisziplinäres Zentrum, Center for Nanoanalysis and Electron Microscopy (CENEM) Graduiertenkolleg 1896/2 In situ Mikroskopie mit Elektronen, Röntgenstrahlen und Rastersonden

Utilized Equipment

FEI Titan Themis 300 (FEI) Lehrstuhl für Werkstoffwissenschaften (Mikro- und Nanostrukturforschung)

Related research project(s)

Growth and stability of anisotropic nanoparticles in liquids (GRK1896-A2) In-situ Characterization of Nanomaterials with Electrons, X-rays/Neutrons and Scanning Probes (GRK 1896) Oct. 1, 2013 - Sept. 30, 2022 In-situ Characterization of Nanomaterials with Electrons, X-rays/Neutrons and Scanning Probes (GRK 1896) Oct. 1, 2013 - Sept. 30, 2022

Involved external institutions

Fraunhofer-Institut für Integrierte Systeme und Bauelementetechnologie (IISB) DE Germany (DE)

How to cite

APA:

Fritsch, B., Hutzler, A., Wu, M., Khadivianazar, S., Vogl, L., Jank, M.,... Spiecker, E. (2021). Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy. Nanoscale Advances, 3(9), 2466 - 2474. https://doi.org/10.1039/D0NA01027H

MLA:

Fritsch, Birk, et al. "Accessing local electron-beam induced temperature changes during in situ liquid-phase transmission electron microscopy." Nanoscale Advances 3.9 (2021): 2466 - 2474.

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